Hydrothermal synthesis autoclave reactor

also called pressure vessel, High Pressure Reactor Autoclave or hydrothermal synthesis autoclave

Information of High Pressure Reactor Autoclave:

Capacity: 20ml 30ml 50ml 75ml 100ml 200ml 400ml 500ml 1000ml 2000ml 

Material: stainless steel SS304, SS316, hastelloy, titanium, cladding plate

Structure of High Pressure Reactor Autoclave:

(1) Jack screw bolt

(2) kettle cover

(3) Butterfly spring pad

(4) Flat Head 
(5) Lining cover

(6) Liner

(7) Bottom cover

(8) Kettle body 

Function of High Pressure Reactor Autoclave: 

The design temperature of this product is 300 °C, design pressure 6Mpa.
There are two types of working temperature according to the different liner in the hydrothermal synthesis reactor. 
Teflon lining ( also called F4, F4): working temperature ≤ 160 °C
PPL lining: temperature ≤ 250 °C

Operation of High Pressure Reactor Autoclave:

1. Loose hexagon head bolt with a wrench, do not have to unload and just move freely.

2. The screw cap is screwed down, and then turn to the 304 filter pad , 304 cover and F4 cover to be taken down.

3. Withstand up the 304 bottom, then remove the 304 F4 liner from upper part of the kettle.

4. Place the reaction materials inside the F4 liner, and ensure that feeding coefficient is less than 0.8.

5. Put F4 liner with reaction materials into the 304 kettle body, and then turn to put on F4 cover,304 cover, 304 filter pad, then tighten the screw cap, and finally tighten the hex head bolt with a wrench.

6. Fix the micro reactors in blast / thermostatic oven, pending the completion of the reaction to remove micro-reactors.

7. After cooling the micro-reactor, repeat the steps 1-3.

8. Transfer the reaction products to the specified container, then wash F4 liner and F4 cover for the next use.

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