50ml Hydrogenation Reaction High Pressure Reactor with PTFE liner Magnetic stirring high temperature and high pressure reactor

The stainless steel micro-reactor is small in size, simple and reliable in structure, temperature setting and digital display. The speed setting is digital. Economical, durable, complete accessories, standard micro DC motor, pressure gauge, explosion-proof device, intake valve, air outlet valve The temperature probe can easily realize the micro reaction test. The kettle body and heater can be completely separated. Greatly facilitates the disassembly of the reactor and improves work efficiency.

1,Stirring motor: High-power motor, powerful and stable.

2,Inlet gas valve: gas inlet and outlet needle valve, connected to 3mm or 6mm ferrule. The quality is reliable.

3,Sampling valve: It is convenient to take samples at any time during the reaction and analyze the reaction process to connect 3mm or 6mm ferrules (optional).

4,Exhaust valve: It is convenient to vacuum and replace the gas before the reaction. After the reaction, it is used as a vent valve.

5,Stainless steel pressure gauge: real-time monitoring of reaction pressure

6,Temperature probe: deep inside the reactor body, real-time monitoring of reaction temperature

1. Pour the reactant into a Teflon liner or PPL liner and ensure that the feed coefficient is less than 0.7.

2. Then place the gasket and place the Teflon bushing or PPL bushing into the matching steel sleeve. Tighten the lid first, then tighten the lid with a screw.

3. If there is a need for ventilation, please connect the ventilation duct first (the ventilation duct needs to be purchased separately).

4. Place the reaction vessel in the heater, put the sensor into the temperature measurement hole, and raise the temperature to the required reaction temperature according to the specified heating rate. (less than the specified safe use temperature). Set the required temperature and speed.

5. If the exhaust is required during the reaction, the valve can be directly opened. If the gas is toxic, it cannot be discharged directly into the air. You need to arrange the recovery bottle yourself. If there is no toxicity, it can be discharged directly into the air.

6. When it is confirmed that the temperature in the autoclave is lower than the boiling point of the solvent of the reactants, the lid can be opened for subsequent operation. When the temperature is lowered by the end of the reaction, it is also strictly operated according to the specified cooling rate to facilitate safety and reaction kettle. Service life.

7. After confirming that the temperature in the kettle is lower than the boiling point of the solvent of the reactant system, first loosen the lid of the kettle with a screw, and then open the lid of the kettle.

8. After each use, the reactor should be cleaned in time to avoid rust. The seals of the kettle body and the kettle lid should be carefully cleaned and protected from damage.

Remember: 1. Do not use the PTFE liner alone in an oven or other heating equipment for cleaning or use. Please use it together with the steel sleeve.

            2. Do not put the kettle with pressure gauge directly in the oven to avoid damage to the pressure gauge.